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Abstract:
In order to study the effect of spark plasma sintering (SPS) technique synthesis SiC-MgB2 on the phase formation, the MgB2 and SiC-MgB2 bulks were fabricated with mixed powders by various SPS synthesis routes. The phase formation processes were investigated with the aid of X-ray diffraction analysis, TEM investigations and sintering theories. The solid-solid reaction between Mg and B powders formed MgB2 at low temperature. As the sintering temperature increases, the reactions of molten Mg with B form MgB2, and simultaneously, the molten Mg promotes the decomposition of SiC and nuclei of Mg2Si may form on the surface of SiC grains; the nascent MgB2 incorporates the carbon into lattice, hereby enhancing the SiC decomposition. The experimental results are in good agreement with the assumed chemical reaction.
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MATERIALS RESEARCH INNOVATIONS
ISSN: 1432-8917
Year: 2014
Issue: 6
Volume: 18
Page: 407-411
JCR Journal Grade:4
CAS Journal Grade:4
Cited Count:
WoS CC Cited Count: 3
SCOPUS Cited Count: 4
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 1