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作者:

Guo, Z. (Guo, Z..) | Suo, H. (Suo, H..) | Sandu, V. (Sandu, V..) | Aldica, G. (Aldica, G..)

收录:

SCIE

摘要:

In order to study the effect of spark plasma sintering (SPS) technique synthesis SiC-MgB2 on the phase formation, the MgB2 and SiC-MgB2 bulks were fabricated with mixed powders by various SPS synthesis routes. The phase formation processes were investigated with the aid of X-ray diffraction analysis, TEM investigations and sintering theories. The solid-solid reaction between Mg and B powders formed MgB2 at low temperature. As the sintering temperature increases, the reactions of molten Mg with B form MgB2, and simultaneously, the molten Mg promotes the decomposition of SiC and nuclei of Mg2Si may form on the surface of SiC grains; the nascent MgB2 incorporates the carbon into lattice, hereby enhancing the SiC decomposition. The experimental results are in good agreement with the assumed chemical reaction.

关键词:

Composite superconductors MgB2 Phase formation Spark plasma sintering

作者机构:

  • [ 1 ] [Guo, Z.]Zhengzhou Univ, Sch Phys & Engn, Zhengzhou 450052, Peoples R China
  • [ 2 ] [Guo, Z.]Beijing Univ Technol, Coll Mat Sci & Engn, Key Lab Adv Funct Mat, Minist Educ, Beijing 100124, Peoples R China
  • [ 3 ] [Suo, H.]Beijing Univ Technol, Coll Mat Sci & Engn, Key Lab Adv Funct Mat, Minist Educ, Beijing 100124, Peoples R China
  • [ 4 ] [Sandu, V.]Natl Inst Mat Phys, Magurele 077125, Romania
  • [ 5 ] [Aldica, G.]Natl Inst Mat Phys, Magurele 077125, Romania

通讯作者信息:

  • [Guo, Z.]Zhengzhou Univ, Sch Phys & Engn, Zhengzhou 450052, Peoples R China

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来源 :

MATERIALS RESEARCH INNOVATIONS

ISSN: 1432-8917

年份: 2014

期: 6

卷: 18

页码: 407-411

JCR分区:4

中科院分区:4

被引次数:

WoS核心集被引频次: 3

SCOPUS被引频次: 4

ESI高被引论文在榜: 0 展开所有

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