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By means of high resolution transmission electron microscopy (HRTEM) and high-angle annular dark-field image technique (HAADF), morphological of plate-shaped sigma phase and interfacial characteristics between plate-shaped sigma phase and gamma phase in Ni-based single crystal superalloys have been studied. On the basis of HRTEM observations, an atomic structural interface between sigma phase and gamma phase with a step has been proposed. sigma Phase has the relationship of [001](gamma)//[11 (2) over bar](sigma), ((2) over bar 20)(gamma)//((1) over bar 10)(sigma), ((2) over bar(2) over bar0)(gamma)//(111)(sigma); [011](gamma)//[110](sigma), (1 (1) over bar1)(gamma)//(00 (1) over bar)(sigma) with the gamma phase. The compositional characteristics of the sigma phase which are rich in more heavy elements, such as W, Re, Cr and Ru, has also been clearly revealed by the HAADF imaging technique and Energy Dispersive X-Ray Spectroscopy (EDS) mapping analysis. (C) 2012 Elsevier B.V. All rights reserved.
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JOURNAL OF ALLOYS AND COMPOUNDS
ISSN: 0925-8388
年份: 2012
卷: 536
页码: 80-84
6 . 2 0 0
JCR@2022
ESI学科: MATERIALS SCIENCE;
JCR分区:1
中科院分区:1