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作者:

Zhang Ping (Zhang Ping.) | Zheng Da-wei (Zheng Da-wei.) | Liu Jing (Liu Jing.) | Zhong Ru-gang (Zhong Ru-gang.) (学者:钟儒刚) | Liu Chun-wei (Liu Chun-wei.) | Guo Xun (Guo Xun.) | Wang Hong (Wang Hong.)

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EI Scopus SCIE PKU CSCD

摘要:

New method for rapid and quantitative analysis of 6-benzylaminopurine (6-BA) residues in sprout beans was studied by using FAST-SPE and portable surface-enhanced Raman spectroscopy (SERS). With homemade sprout bean samples as blank control, 6-BA solutions extracted from inserted-treatment samples showed typical characteristic Raman peaks at 1 002 cm(-1) tested by SERS, and normalized 1 002 cm(-1) intensities had a good linear relationship with gradient concentrations of 6-BA insert-standard solutions. The high concentration linear range was 0.5 similar to 14 mu g . mL(-1), and the low one was 0.1 similar to 2 mu g . mL(-1). The quantitative detection limit was down to 0.02 mg . kg(-1) that was below the maximum allowable residues (MAL) of 0.2 mg . kg(-1) in related National Standard. The recoveries were 82.3%similar to 95.1% and the RSD was below 5%. This method with portable equipment and simple pre-treatment showed good reproducibility, short test time-consuming and easy operating, and thus it would provide efficient and sensitive solutions for large-scale on-site and rapid detections.

关键词:

6-benzylaminopurine Plant growth regulator Rapid detection Residue Surface-enhanced Raman spectroscopy

作者机构:

  • [ 1 ] [Zhang Ping]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China
  • [ 2 ] [Zheng Da-wei]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China
  • [ 3 ] [Liu Jing]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China
  • [ 4 ] [Zhong Ru-gang]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China
  • [ 5 ] [Liu Chun-wei]OptoTrace Technol Inc, Suzhou 215125, Peoples R China
  • [ 6 ] [Guo Xun]OptoTrace Technol Inc, Suzhou 215125, Peoples R China
  • [ 7 ] [Wang Hong]OptoTrace Technol Inc, Suzhou 215125, Peoples R China

通讯作者信息:

  • 钟儒刚

    [Zhong Ru-gang]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China

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来源 :

SPECTROSCOPY AND SPECTRAL ANALYSIS

ISSN: 1000-0593

年份: 2012

期: 5

卷: 32

页码: 1266-1269

0 . 7 0 0

JCR@2022

ESI学科: CHEMISTRY;

ESI高被引阀值:233

JCR分区:4

中科院分区:4

被引次数:

WoS核心集被引频次: 8

SCOPUS被引频次:

ESI高被引论文在榜: 0 展开所有

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中文被引频次:

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