• 综合
  • 标题
  • 关键词
  • 摘要
  • 学者
  • 期刊-刊名
  • 期刊-ISSN
  • 会议名称
搜索

作者:

Cui Yuntao (Cui Yuntao.) | Wang Jinshu (Wang Jinshu.) (学者:王金淑) | Liu Wei (Liu Wei.) | Zang Lei (Zang Lei.) | Li Shuo (Li Shuo.) | Li Zhen (Li Zhen.) | Ye Linghan (Ye Linghan.) | Zhou Meiling (Zhou Meiling.)

收录:

EI Scopus SCIE PKU CSCD

摘要:

The spherical tungsten powder was fabricated by spray-drying method combined with hydrogen reduction using ammonium metatungstate (AMT) as raw materials. The powder morphology, mean particle size, particle size distribution and phase transformation process of reduction were characterized by SEM, TEM, XRD and laser diffraction particle size analyzer, respectively. Results show that the morphology of the powder prepared by spray drying is hollow sphere, and both of AMT and WO3 powder has similar good spherical structure with smooth surface. TEM results indicate that the process parameters, such as the slurry concentration, compressed air flow rate, and liquid feeding rate, play important roles in controlling the performance of AMT microspheres, such as the size distribution. It is found that calcination has no effect on the particle morphology and phase composition. The mean size is increased with the increase of the slurry concentration and compressed air flow rate, but the size distribution changes slightly with different liquid feed rates. The X-ray diffraction patterns indicate that alpha-W phase is obtained after reduction at 550 degrees C for 2 h in hydrogen atmosphere, but WO3 still exists; after reduction at 750 degrees C for 2 h, WO3 disappears, and a-W phase exists in the powder.

关键词:

cathode materials reduction spherical tungsten powder spray-drying

作者机构:

  • [ 1 ] [Cui Yuntao]Beijing Univ Technol, Coll Mat Sci & Engn, Key Lab New Funct Mat, Minist Educ, Beijing 100124, Peoples R China

通讯作者信息:

  • [Cui Yuntao]Beijing Univ Technol, Coll Mat Sci & Engn, Key Lab New Funct Mat, Minist Educ, Beijing 100124, Peoples R China

电子邮件地址:

查看成果更多字段

相关关键词:

来源 :

RARE METAL MATERIALS AND ENGINEERING

ISSN: 1002-185X

年份: 2011

期: 3

卷: 40

页码: 507-510

0 . 7 0 0

JCR@2022

ESI学科: MATERIALS SCIENCE;

ESI高被引阀值:290

JCR分区:4

中科院分区:4

被引次数:

WoS核心集被引频次: 5

SCOPUS被引频次:

ESI高被引论文在榜: 0 展开所有

万方被引频次:

中文被引频次:

近30日浏览量: 2

在线人数/总访问数:369/2896173
地址:北京工业大学图书馆(北京市朝阳区平乐园100号 邮编:100124) 联系我们:010-67392185
版权所有:北京工业大学图书馆 站点建设与维护:北京爱琴海乐之技术有限公司