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作者:

Ni, Cheng-Liang (Ni, Cheng-Liang.) | Song, Xiao-Hui (Song, Xiao-Hui.) | Yan, Hong (Yan, Hong.) (学者:闫红) | Song, Xiu-Qing (Song, Xiu-Qing.) | Zhong, Ru-Gang (Zhong, Ru-Gang.) (学者:钟儒刚)

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摘要:

Diethyl 2,6-dimethyl-4-aryl-4H-pyran-3,5-dicarboxylates (1) have been synthesized by the reaction of aryl aldehyde and 1,3-diketone catalyzed by ZnCl2 under ultrasound irradiation. The effects of changes in the ultrasonic power, temperature, and reaction time are discussed. With the optimized reaction conditions, various aryl aldehydes were used to synthesize 4H-pyrans (1) under the influence of ultrasound irradiation. Compared with the conventional thermal methods, the remarkable advantages of this method are the simple experimental procedure, shorter reaction time and high yield of product. (C) 2009 Elsevier B.V. All rights reserved.

关键词:

Aryl aldehyde 4-Aryl-4H-pyran Synthesis 1,3-Diketone Ultrasound

作者机构:

  • [ 1 ] [Ni, Cheng-Liang]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China
  • [ 2 ] [Song, Xiao-Hui]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China
  • [ 3 ] [Yan, Hong]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China
  • [ 4 ] [Song, Xiu-Qing]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China
  • [ 5 ] [Zhong, Ru-Gang]Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing 100124, Peoples R China

通讯作者信息:

  • 闫红

    [Yan, Hong]Beijing Univ Technol, Coll Life Sci & Bioengn, Pingleyuan St 100, Beijing 100124, Peoples R China

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来源 :

ULTRASONICS SONOCHEMISTRY

ISSN: 1350-4177

年份: 2010

期: 2

卷: 17

页码: 367-369

8 . 4 0 0

JCR@2022

ESI学科: CHEMISTRY;

JCR分区:1

中科院分区:1

被引次数:

WoS核心集被引频次: 42

SCOPUS被引频次: 40

ESI高被引论文在榜: 0 展开所有

万方被引频次:

中文被引频次:

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