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摘要:
Spark plasma sintering (SPS) and conventional sintering techniques were used to fabricate sintered Nd-Fe-B permanent magnets. The corrosion behaviors of both magnets in sodium chloride (NaCl), sodium hydroxide (NaOH), and sulfuric acid (H(2)SO(4)) solutions were studied. The weight-loss curves indicate that both magnets exhibit passive behavior in alkaline solution and dissolve actively in acid solution. SEM observations show that the conventional sintered Nd-Fe-B magnets exhibit typical intergranular corrosion. In the SPS magnet, however, intergranular corrosion through the Nd-rich phase is suppressed effectively due to the unique microstructure of the magnets, i.e., the grain size of the Nd(2)Fe(14)B main phase is fine and uniform, and the fine Nd-rich phase does not form along the grain boundaries of main phase as with conventional magnets, but agglomerates into the triple junctions. As a result, the SPS Nd-Fe-B magnets possess excellent corrosion resistance.
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CORROSION
ISSN: 0010-9312
年份: 2009
期: 7
卷: 65
页码: 501-504
1 . 6 0 0
JCR@2022
ESI学科: MATERIALS SCIENCE;
JCR分区:1
中科院分区:1