An　array　of　novel　chiral　aromatic　heterocyclic　macrocycles,　which　may　show　potential　enantiomeric　recognition　to　variable　D-　and　L-amino　acids,　were　synthesized　in　acceptable　yield.　The　desired　macrocycles　3a-c　and　4a-c　were　obtained　via　the　condensation　reaction　of　chiral　diamine　intermediates　2a-c　with　2,5-bis(o-chloroformylphenyl)-1,3,4-triazole　5　in　a　presence　of　Et3N　in　a　highly　diluted　dichloromethane　solution　at　room　temperature.