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SnO2-TiO2 thin films were deposited on the activated glassy carbon electrodes by vacuum coating method. Au-Pt/SnO2-TiO2/GC composite electrode was prepared by reducing HAuCl4 and H2PtCl6 mixture Solution and sediment Au-Pt bimetallic nanoparticles successively on the SnO2-TiO2/GC. The effect of SnO,-TiO, film support on the electrocatalytic properties of Au-Pt nanoparticles was characterized via cyclic voltograme method. The morphological and structural properties of Au-Pt nanoparticles self-assembled on SnO2-TiO2 film were characterized via Scanning Electron Microscope and X-ray Photoelectron Spectroscopy. The results show that the compact and uniformed 10 nm Au-Pt nanoparticles were self-assembled on SSnO2-TiO2 film. The ability of anti-CO poisoning was enhanced with the function of SnO2-TiO2 support. The form of Au-Pt alloy enhanced the electrocatalytic oxidation of methanol in acidic system. Furthermore, the increase of d vacancy with the function of SnO2-TiO2 support improved the stability and catalytic property of Au-Pt bimetallic nanoparticles.
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