收录:
摘要:
BaxSr1-xTiO3(BST) film has a good foreground as an important ferroelectric film in DRAM, pyroelectric infrared detector, film-ceramic capacitor and film sensor, etc. due to strong nonlinear dielectricity, small leak current and fatigue characteristics. Ba0.7Sr0.3TiO3 ferroelectric films were prepared by water-based sol-gel process in this paper. By changing techniques condition of preparation, techniques that homogeneous and crack-less ferroelectric films were prepared with water-based sol-gel process was searched. The structure and properties of sol-gel and the films were analyzed by available testing measure such as optical microscopy (OM), XRD, SEM and TEM. The influences of hydrolysis-polymerization process and degree of hydrolysis on production of sol-gel were investigated. The effects of process condition on properties of films were studied. The influences of heat treat condition to crystallinity were discussed. The results show that the higher concentration of water-based precursor solution is beneficial to form a uniform film. The optimum processing parameters for preparing films are as follows: concentration of precursor solution is 0.56 mol/L; pH value is 5.5; aging time is 48 similar to 72 h. Film sample with good performance can be obtained under the optimum conditions. The XRD analysis indicates that film had been perovskite after 650 degrees C treatment.
关键词:
通讯作者信息:
电子邮件地址: