收录:
摘要:
A gas microinjector system was set up in an environmental scanning electron microscope (ESEM) to create an oxygen atmosphere around the alumina samples for the charging compensation under a pressure between 2 x 10(-5) Pa similar to 2 x 10(-2) Pa. At low pressures, the skin effect of the electron scattering can be degraded, which results in improvement of the imaging contrast and increase of the signal/noise ratio. The sample current (I-sc) and the Duane-Hunt limit were measured to evaluate the charging effect.
关键词:
通讯作者信息:
电子邮件地址:
来源 :
SCANNING
ISSN: 0161-0457
年份: 2006
期: 5
卷: 28
页码: 289-293
ESI学科: CHEMISTRY;
JCR分区:4
归属院系: