• 综合
  • 标题
  • 关键词
  • 摘要
  • 学者
  • 期刊-刊名
  • 期刊-ISSN
  • 会议名称
搜索

作者:

Zhang, GZ (Zhang, GZ.) | Zhang, LP (Zhang, LP.) | Wang, C (Wang, C.) | Zhang, HX (Zhang, HX.) | Zhou, ML (Zhou, ML.) | Zhong, TX (Zhong, TX.)

收录:

SCIE PKU CSCD

摘要:

WO3 and carbon mixed powder can be in-sit synthesized to compact WC bulk by spark plasma sintering. The phase, the density and the microstructure of the. sample synthesized at different temperatures have been studied. The mechanism of synthesis was analyzed. With the rising of the synthesis temperatures, WO3 can be rapidly reduced to WO2.72, WO2 and W, then carbonized to W2C and WC. Each step of the synthesis was overlapped. When the temperature was lower than 1118 degrees C, it is occur phase changes, but the density does not change significantly. When the temperature was higher than 1118 degrees C, a small amount of the remained W2C disappears, the sample begins to sinter, the density of the bulk is near the theoretical density. The microstructure of the sample changes with the synthesis temperatures. WO2.72 was rod shape, whereas WO3, WO2, W, W2C, WC were granular. The particle sizes grow from 0.2 mu m to about 0.5 mu m. CO2 gives off in the earlier stage Of WO3 reducing, CO gives off in the later stage during SPS synthesis. WO2.9 does not appear during the reducing reaction.

关键词:

cemented carbides in-situ synthesis SPS WC tungsten oxide

作者机构:

  • [ 1 ] Minist Educ, Key Lab Adv Funct Mat, Beijing 100022, Peoples R China

通讯作者信息:

  • [Zhang, GZ]Beijing Univ Technol, Beijing 100022, Peoples R China

电子邮件地址:

查看成果更多字段

相关关键词:

来源 :

RARE METAL MATERIALS AND ENGINEERING

ISSN: 1002-185X

年份: 2005

期: 11

卷: 34

页码: 1743-1746

0 . 7 0 0

JCR@2022

ESI学科: MATERIALS SCIENCE;

JCR分区:2

被引次数:

WoS核心集被引频次: 2

SCOPUS被引频次:

ESI高被引论文在榜: 0 展开所有

万方被引频次:

中文被引频次:

近30日浏览量: 1

归属院系:

在线人数/总访问数:152/4298613
地址:北京工业大学图书馆(北京市朝阳区平乐园100号 邮编:100124) 联系我们:010-67392185
版权所有:北京工业大学图书馆 站点建设与维护:北京爱琴海乐之技术有限公司