Polycarboxylate　superplasticizer　(PCE)　was　synthesized　in　non-aqueous　system　to　achieve　the　rapid　transportation　and　convenient　preparation.　The　results　showed　that,　PCE　using　isopentenyl　polyethylene　glycol　(TPEG)　or　isobutenyl　polyethylene　glycol　(PEG)　as　macromonomer　exhibited　excellent　paste　fluidities　and　retaining　properties　at　80　degrees　C　and　75　degrees　C,　respectively.　Fourier　Transform　infrared　spectroscopy　(FTIR)　measurement　confirmed　the　polymerization　between　monomers.　The　synthesized　PCE　as　solid　state　was　dissolved　into　water　to　prepare　the　PCE　solution,　and　its　cement　application　performances　were　studied　systematically.　The　results　showed　that　PCEs　with　good　paste　fluidity　retentions　exhibited　the　longest　final　setting　time　and　the　shortest　setting　time　interval.　The　hydration　heat　results　showed　that　PCEs　with　good　fluidity　properties　can　significantly　delay　the　hydration　process　and　lower　the　hydration　heat.