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作者:

Yang Shuai (Yang Shuai.) | Luo Yunjing (Luo Yunjing.) (学者:罗云敬) | Mu Lei (Mu Lei.) | Yang Youyou (Yang Youyou.) | Yang Yongtan (Yang Yongtan.)

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摘要:

An liquid chromatography-tandem mass spectrometry method coupled with a stable isotope dilution assay was established for the simultaneous detection of 17 mycotoxins and their derivatives (aflatoxins B1 , B2 , G1 , G2 , M1 , and M2 ; fumonisins B1 and B2 ; ochratoxin A; zearalenone; zearalanone; α-zearalanol; α-zearalenol; T-2 toxin; deoxynivalenol; deepoxy-deoxynivalenol; and sterigmatocystin) in milk and dairy products. The mycotoxins were extracted with acidified acetonitrile and the lipids were removed using a Captiva EMR-lipid column. The average recoveries of the target compounds from samples spiked at three different concentrations were 67-102%, and the relative standard deviations of the peak areas were less than 10%. Limits of quantification (S/N = 10) of 0.004-1.25 μg/kg were achieved, which are significantly lower than the maximum levels allowed in various countries and regions for each regulated mycotoxin. Milk and yogurt products from local markets and e-commercial platforms were analyzed using the optimized method. The screening showed that aflatoxin M1 , deoxynivalenol, fumonisins B1 and B2 , and zearalenone could be found in milk and yogurt products, especially those products also containing grains or jujube ingredients, indicating that there is a risk of mycotoxins in dairy products.

关键词:

multimycotoxins isotope dilution risk assessment dairy

作者机构:

  • [ 1 ] [Yang Shuai]China Oil & Foodstuffs Corporation (COFCO) Nutrition and Health Research Institute, Beijing, P. R. China
  • [ 2 ] [Luo Yunjing]College of Life Science and Bioengineering, Beijing University of Technology, Beijing, P. R. China
  • [ 3 ] [Mu Lei]China Oil & Foodstuffs Corporation (COFCO) Nutrition and Health Research Institute, Beijing, P. R. China
  • [ 4 ] [Yang Youyou]China Oil & Foodstuffs Corporation (COFCO) Nutrition and Health Research Institute, Beijing, P. R. China
  • [ 5 ] [Yang Yongtan]Academy of State Administration of Grain, Beijing, P. R. China

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来源 :

Journal of separation science

ISSN: 1615-9314

年份: 2021

期: 4

卷: 44

页码: 782-792

3 . 1 0 0

JCR@2022

ESI学科: CHEMISTRY;

ESI高被引阀值:96

JCR分区:2

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WoS核心集被引频次: 0

SCOPUS被引频次: 15

ESI高被引论文在榜: 0 展开所有

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