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摘要:
Uniform scandium doped tungsten powder was prepared by sol-gel method combined with reduction process, and then the scandium doped impregnated cathode was successfully prepared by microwave sintering. The characteristics of Sc-doped tungsten powder, the microstructure of cathode sponge matrix, the emission properties, and the surface behavior of the active substance were analyzed. The result shows that the scandium doped tungsten powder has the average size of around 1 mu m and Sc element is uniformly distributed. The morphology of the sponge skeleton is spherical, the pore distribution is uniform, the average pore diameter is about 0.46 mu m, and scandium is evenly distributed in the matrix. The cathode prepared by the microwave sintering method exhibits good emission properties, e.g., the current density of this cathode reaches 137.59 A/cm(2) at 950 degrees C-b, and the emission slope is 1.431. The atomic ratio of Ba:Sc:O on the cathode surface is 1.8:1:2.2 after activation, and a large amount of nanoparticles are present on the cathode surface, which promotes emission of the cathode.
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来源 :
RARE METAL MATERIALS AND ENGINEERING
ISSN: 1002-185X
年份: 2020
期: 5
卷: 49
页码: 1766-1772
0 . 7 0 0
JCR@2022
ESI学科: MATERIALS SCIENCE;
ESI高被引阀值:169