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作者:

Liu Wei (Liu Wei.) | Li Junhui (Li Junhui.) | Wang Jinshu (Wang Jinshu.) (学者:王金淑) | Zhou Fan (Zhou Fan.) | Yang Yunfei (Yang Yunfei.) | Pan Zhaoliu (Pan Zhaoliu.) | Wu Hao (Wu Hao.) | Li Shilei (Li Shilei.)

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EI SCIE CSCD

摘要:

Uniform scandium doped tungsten powder was prepared by sol-gel method combined with reduction process, and then the scandium doped impregnated cathode was successfully prepared by microwave sintering. The characteristics of Sc-doped tungsten powder, the microstructure of cathode sponge matrix, the emission properties, and the surface behavior of the active substance were analyzed. The result shows that the scandium doped tungsten powder has the average size of around 1 mu m and Sc element is uniformly distributed. The morphology of the sponge skeleton is spherical, the pore distribution is uniform, the average pore diameter is about 0.46 mu m, and scandium is evenly distributed in the matrix. The cathode prepared by the microwave sintering method exhibits good emission properties, e.g., the current density of this cathode reaches 137.59 A/cm(2) at 950 degrees C-b, and the emission slope is 1.431. The atomic ratio of Ba:Sc:O on the cathode surface is 1.8:1:2.2 after activation, and a large amount of nanoparticles are present on the cathode surface, which promotes emission of the cathode.

关键词:

scandium dispenser cathode tungsten thermionic emission microwave sintering

作者机构:

  • [ 1 ] [Liu Wei]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China
  • [ 2 ] [Li Junhui]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China
  • [ 3 ] [Wang Jinshu]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China
  • [ 4 ] [Zhou Fan]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China
  • [ 5 ] [Yang Yunfei]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China
  • [ 6 ] [Pan Zhaoliu]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China
  • [ 7 ] [Wu Hao]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China
  • [ 8 ] [Li Shilei]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China

通讯作者信息:

  • [Liu Wei]Beijing Univ Technol, Minist Educ, Key Lab Adv Funct Mat, Beijing 100124, Peoples R China

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来源 :

RARE METAL MATERIALS AND ENGINEERING

ISSN: 1002-185X

年份: 2020

期: 5

卷: 49

页码: 1766-1772

0 . 7 0 0

JCR@2022

ESI学科: MATERIALS SCIENCE;

ESI高被引阀值:169

被引次数:

WoS核心集被引频次: 11

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ESI高被引论文在榜: 0 展开所有

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