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摘要:
W alloys prepared via oxide dispersion strengthening have shown enhanced mechanical performance. In this paper, W-1.10 vol% Zr-2.00 vol% Y2O3 (WZY) and W-1.10 vol% Zr-2.00 vol% Er2O3 (WZE) were fabricated to investigate the effects of formation of complex oxide dispersions on mechanical properties and microstructure of multi-doped W alloys. By controlling the atomic ratio of added ZrH2 and rare earth oxides through composition design, the goal of complete formation of complex oxide particles with pyrochlore structure (A(2)B(2)O(7)) was achieved. Electron probe microanalysis (EPMA) and transmission electron microscopy (TEM) results showed that these dispersion particles in WZY and WZE were Y2Zr2O7 and Er2Zr2O7, respectively. Moreover, microstructure analysis showed that Er 2 Zr2O7 exhibited smaller size, higher number density and more homogenous distribution compared to Y2Zr2O7, which led to finer grains of WZE (0.58 +/- 0.03 mu m) compared to WZY (1.34 +/- 0.29 mu m). Finer microstructure including smaller grains and dispersion particles of WZE contributed to its higher strength and better ductility. Furthermore, the formation mechanism of complex oxide dispersion particles was discussed in detail.
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来源 :
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
ISSN: 0921-5093
年份: 2021
卷: 824
6 . 4 0 0
JCR@2022
ESI学科: MATERIALS SCIENCE;
ESI高被引阀值:116
JCR分区:1