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The DyHx nano-powders were prepared by hydrogen arc plasma method, and then the mixed of DyHx nano-powders and micron boron were sintered by spark plasma sintering (SPS) method to fabricate high-properties polycrystalline DyB6 bulk. The influence of SPS sintering temperature on the microstructure and property was investigated. It is shown that the pure phase DyB6 bulk can be easily fabricated by SPS when the sintering temperature is 1275°C. The values of density, Vickers hardness and bend strength respectively reach 5.191g/cm3, 23.32GPa and 112.8MPa when the sample was sintered at 1425°C and 60MPa. Thermionic emission measurement of the sample was performed. The emission current density of the DyB6 is 3.6A/cm2 at 1933K.
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