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Sphere-like and rod-like Eu2O3 and Sm2O3 polycrystalline nanoparticles were fabricated by using a surfactant-and ultrasonic-assisted precipitation strategy. The physical properties of these nanomaterials were characterized by means of transmission electron microscopic (TEM), selected area electron diffraction (SAED), X-ray diffraction (XRD), nitrogen adsorption-desorption, and ultraviolet-visible diffuse reflection spectroscopic (UV-Vis DRS) techniques. It is shown that the sphere-like body-centered cubic Eu2O3 and monoclinic Sm2O3 nanoparticles obtained with sodium dodecylsulfate as surfactant and the rod-like orthorhombic Eu2O3 and body-centered cubic Sm2O3 nanoparticles fabricated with polyvinylpyrrolidone as surfactant possessed a BET surface area of 44~49 and 34~37m2/g, respectively. In addition to a stronger absorption of UV light (λ2O3 and Sm2O3 samples exhibited different absorption of visible light (390nm
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