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作者:

Zhang, Dong-Tao (Zhang, Dong-Tao.) (学者:张东涛) | Xu, Gang (Xu, Gang.) | He, Jian (He, Jian.) | Yang, Jian-Jun (Yang, Jian-Jun.) | Yue, Ming (Yue, Ming.) (学者:岳明) | Liu, Wei-Qiang (Liu, Wei-Qiang.) (学者:刘卫强) | Zhang, Jiu-Xing (Zhang, Jiu-Xing.)

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摘要:

Bulk nanocrystalline Sm2Co17sintered magnet was prepared by high energy ball-milling and spark plasma sintering (SPS) technique. Structure and magnetic properties of the powders and magnet were studied. XRD patterns show that annealed at low temperature (7structure. When annealed temperature is above 1023K, the main phase is Th2Zn17structure. With increasing the annealed temperature from 923-1223K, the coercivity of the powders decrease from 0.99-0.12T. The sintered magnet also exhibits TbCu7structure after SPS process. TEM observation indicates that the average grain size of the magnet is about 35 nm. Magnetic measurement of the sintered magnet shows that the remanence is 0.65T and the coercivity reaches 0.87T; The magnet exhibits a better thermal stability with a remanence of 0.6T and a coercivity of 0.32T at 573K.

关键词:

Annealing Ball milling Coercive force Magnets Nanocrystalline powders Nanocrystals Powders Remanence Sintering Spark plasma sintering Temperature

作者机构:

  • [ 1 ] [Zhang, Dong-Tao]The Key Laboratory of Advanced Functional Materials Ministry of Education, Beijing University of Technology, Beijing 100124, China
  • [ 2 ] [Xu, Gang]The Key Laboratory of Advanced Functional Materials Ministry of Education, Beijing University of Technology, Beijing 100124, China
  • [ 3 ] [He, Jian]Magnetic Material Testing Laboratory, National Institute of Metrology, Beijing 100013, China
  • [ 4 ] [Yang, Jian-Jun]The Key Laboratory of Advanced Functional Materials Ministry of Education, Beijing University of Technology, Beijing 100124, China
  • [ 5 ] [Yue, Ming]The Key Laboratory of Advanced Functional Materials Ministry of Education, Beijing University of Technology, Beijing 100124, China
  • [ 6 ] [Liu, Wei-Qiang]The Key Laboratory of Advanced Functional Materials Ministry of Education, Beijing University of Technology, Beijing 100124, China
  • [ 7 ] [Zhang, Jiu-Xing]The Key Laboratory of Advanced Functional Materials Ministry of Education, Beijing University of Technology, Beijing 100124, China

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来源 :

Journal of Functional Materials

ISSN: 1001-9731

年份: 2009

期: 6

卷: 40

页码: 909-911

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