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摘要:
CeO2 precursors were prepared by the homogeneous precipitation method, hydrothermal synthesis method and hydrothermal precipitation coupling method using urea as a precipitator. The results indicated that urea was a reserve resource of CO32-·CeO2 precursors were orthorhombic Ce2O (CO3)2·H2O, hexagonal Ce(OH) (CO3), orthorhombic CeO (CO3)2·H2O respectively when the homogeneous precipitation method, hydrothermal synthesis method and hydrothermal precipitation coupling method were used. The synthesis technology had a great effect on the precursors. Different precursors were synthesized through various processes and mechanisms. When heated up to the temperature of 500°C, the precursors were all finally changed into face centred cubic CeO2 powders.
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来源 :
Journal of Chemical Industry and Engineering (China)
ISSN: 0438-1157
年份: 2006
期: 9
卷: 57
页码: 2241-2244