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Melt-SHS (Self-propagating High-temperature Synthesis) was used for the preparation of Al–5Ti–1B master alloy. The quality ratio of Ti powder/TiO2in initial powder mixture was varied from 0:1 to 1:0. The AES, XRD and SEM were applied to evaluate the microstructure and phase componet. The results showed that the Al-5Ti-1B master alloy could be successful produced by the reaction of Al powder, TiO2and H3BO3in Al melt, while the reaction rate was slow. The microstructure mainly presents the TiAl3particles with long strip shape. A significant improvement was noted both in reaction rate and in the grain refining efficiency when Ti powder was added to the reactants and the optimized ratio of Ti powder/TiO2was 2:3. The TiAl3particles were reduced and the grain refining efficiency turned bad when Ti powder was totally used to supply Ti. © 2017 Trans Tech Publications, Switzerland.
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ISSN: 0255-5476
年份: 2017
卷: 877
页码: 121-126
语种: 英文
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