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The densification, microstructure and hardness of molybdenum prepared by spark plasma sintering (SPS) were investigated. SPS is an advanced rapid sintering technique with a lower temperature and shorter time, compared with other sintering techniques. The molybdenum sintered by SPS at 180-500 °C lower than by CIP-S and HP and in holding time of 3 min obtained relative density of 95.2%-97.9% and hardness HV20-HV75 higher than that by other sintering techniques. The density of molybdenum sintered by SPS increases and the hardness of molybdenum decreases with the temperature increasing. The molybdenum sintered at lower temperature by SPS having higher hardness is due to fine grain strengthening. The fracture mode of SPS sintered molybdenum belongs to brittle intercrystalline fracture.
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