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The synthetic method of (2 - azido - 1,1 - dinitroethyl) benzene derivatives was discussed in detail. By the hydroxymethylation, inflation and azidation of substituted phenyl dinitromethane potassium salt, the target compounds, such as 3 - nitro - (2 - azido - 1,1 - dinitroethyl) benzene(4b), 4 - nitro - (2 - azido - 1,1 - dinitroethyl)benzene(4c), m - bis(2 - azido - 1,1 - dinitroethyl)benzene(10) and p - bis(2 - azido - 1,1 - dinitroethyl)benzene(15), were obtianed.
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