Synthesis of 3,9-diazatetraasteranes - 文章详情页

作者：

Zhu, X. (Zhu, X..) | Ni, C. (Ni, C..) | Song, X. (Song, X..) | Yan, H. (Yan, H..) | Zhong, R. (Zhong, R..)

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摘要：

3,9-Diazahexacyclo[6.4.0.02,7.04,11.0　5,10]dodecanes　were　synthesized　by　a　head-to-tail　[2+2]　photocycloaddition　of　1,4-dihydropyridines.　Various　factors　such　as　solvents,　the　concentrations　of　1,4-dihydropyridine,　wavelength　of　UV　and　reaction　time,　were　studied　in　details.　An　efficient　method　of　synthesizing　3,9-diazatetraasteranes　was　found,　and　12　compounds　were　obtained　and　characterized　by　IR,　1H　NMR,　13C　NMR,　MS　and　HRMS　techniques.

关键词：

1-4-dihydropyridine; 3-9-diazatetraasterane; [2+2] photocycloaddition

作者机构：

[ 1 ] [Zhu, X.]College of Life Sciences and Bioengineering, Beijing University of Technology, Beijing 100124, China
[ 2 ] [Ni, C.]College of Life Sciences and Bioengineering, Beijing University of Technology, Beijing 100124, China
[ 3 ] [Song, X.]College of Life Sciences and Bioengineering, Beijing University of Technology, Beijing 100124, China
[ 4 ] [Yan, H.]College of Life Sciences and Bioengineering, Beijing University of Technology, Beijing 100124, China
[ 5 ] [Zhong, R.]College of Life Sciences and Bioengineering, Beijing University of Technology, Beijing 100124, China

通讯作者信息：

[Zhu, X.]College of Life Sciences and Bioengineering, Beijing University of Technology, Beijing 100124, China

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