Nanoparticle　agglomeration　in　a　polymer　matrix　is　often　an　intractable　issue　for　the　advancement　of　nanohybrid　membranes,　and　achieving　scaled-up　production　also　requires　the　development　of　simpler,　more　efficient　and　more　environmentally　friendly　fabrication　mechanisms　than　what　are　currently　used.　Herein,　we　report　a　hight-hroughput　methodology　for　fabricating　nanodisperse　hybrid　membranes　by　directly　atomizing　the　oligomer　(no　solvent)　and　a　crosslinker　solution　doped　with　nanoparticles　and　then　allowing　the　nanoparticles　to　crosslink　rapidly　on　a　rotating　substrate　surface.　It　has　been　proven　that　a　robust　and　defect-free　nanohybrid　membrane　can　be　fabricated　within　3　min,　requiring　almost　2-3　orders　of　magnitude　less　time　than　conventional　solution-coating　technologies　(200-6700　min).　Moreover,　various　nanoparticles　can　be　dispersed　uniformly　on　a　nanometer　scale　into　the　selective　layer　by　the　atomization　synergistic　effect,　and　the　resulting　membranes　exhibit　excellent　overall　performance　and　good　stability　for　biobutanol　recovery.　To　further　demonstrate　the　universality　of　this　technique,　this　work　has　been　successfully　extended　from　flat-sheet　substrates　to　hollow-fiber　and　tubular　substrates.　In　addition,　the　environmental　impact　of　nanohybrid　membrane-making　processes　has　been　evaluated　quantitatively　to　further　illustrate　the　greenness　of　this　facile　approach.