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作者:

Liu, Xiao-mei (Liu, Xiao-mei.) | He, Ding-yong (He, Ding-yong.) (学者:贺定勇) | Wang, Yi-ming (Wang, Yi-ming.) | Zhou, Zheng (Zhou, Zheng.) (学者:周正) | Wang, Guo-hong (Wang, Guo-hong.) | Tan, Zhen (Tan, Zhen.) | Wang, Zeng-jie (Wang, Zeng-jie.)

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EI Scopus SCIE

摘要:

Hydroxyapatite (HA) is one of the most important bioceramic materials used in medical implants. The structure of HA coatings is closely related to their manufacturing process. In the present study, HA coatings were deposited on Ti-6Al-4V substrate by micro-plasma spraying. Results show that three distinct HA coatings could be obtained by changing the spraying power from 0.5 to 1.0 kW and spraying stand-off distance from 60 to 110 mm: (1) high crystallinity (93.3%) coatings with porous structure, (2) high crystallinity coatings (86%) with columnar structure, (3) higher amorphous calcium phosphate (ACP, 50%) coatings with dense structure. The in-flight particles melting state and splat topography was analyzed to better understand the formation mechanism of three distinct HA coatings. Results show that HA coatings sprayed at low spraying power and short stand-off distance exhibit high crystallinity and porosity is attributed to the presence of partially melted particles. High crystallinity HA coatings with (002) crystallographic texture could be deposited due to the complete melting of the in-flight particles and low cooling rate of the disk shape splats under higher spraying power and shorter SOD. However, splashed shape splats with relative high cooling can be provided by increasing SOD, which leads to the formation of ACP.

关键词:

hydroxyapatite coatings in-flight particles micro-plasma spraying texture

作者机构:

  • [ 1 ] [Liu, Xiao-mei]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing, Peoples R China
  • [ 2 ] [He, Ding-yong]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing, Peoples R China
  • [ 3 ] [Wang, Yi-ming]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing, Peoples R China
  • [ 4 ] [Zhou, Zheng]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing, Peoples R China
  • [ 5 ] [Tan, Zhen]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing, Peoples R China
  • [ 6 ] [He, Ding-yong]Beijing Univ Technol, Beijing Engn Res Ctr Ecomat & LCA, Beijing, Peoples R China
  • [ 7 ] [Zhou, Zheng]Beijing Univ Technol, Beijing Engn Res Ctr Ecomat & LCA, Beijing, Peoples R China
  • [ 8 ] [Wang, Guo-hong]Beijing Univ Technol, Beijing Engn Res Ctr Ecomat & LCA, Beijing, Peoples R China
  • [ 9 ] [Wang, Zeng-jie]Beijing Univ Technol, Beijing Engn Res Ctr Ecomat & LCA, Beijing, Peoples R China

通讯作者信息:

  • 贺定勇

    [Liu, Xiao-mei]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing, Peoples R China;;[He, Ding-yong]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing, Peoples R China;;[He, Ding-yong]Beijing Univ Technol, Beijing Engn Res Ctr Ecomat & LCA, Beijing, Peoples R China

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来源 :

JOURNAL OF THERMAL SPRAY TECHNOLOGY

ISSN: 1059-9630

年份: 2018

期: 4

卷: 27

页码: 667-679

3 . 1 0 0

JCR@2022

ESI学科: MATERIALS SCIENCE;

ESI高被引阀值:131

被引次数:

WoS核心集被引频次: 13

SCOPUS被引频次: 19

ESI高被引论文在榜: 0 展开所有

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