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A single alkali fusion regent (Na2O2) was used for decomposition of waste phosphors in this study. After flooding, alkali separation, extraction by hydrochloric acid, ammonia separation, removal of silicon and rare earth oxalate precipitation, the gravimetric method was used to determination of total rare earth oxide in the waste phosphors. Recoveries and precision experiments were investigated in the research. The measuring range of the rare earth elements was 10.00%~70.00% and the recovery at 99.60%~100.40% was obtained. The method is simple, accurate and applicability. © 2016, Editorial Office of "Chinese Rare Earths". All right reserved.
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