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Nickel and tungsten composite coatings were prepared by molten salt electrodeposition. Micromorphology, grain size and ratio of low angle grain boundaries of the coatings were characterized by means of scanning electronic microscopy (SEM) and electron backscattered diffraction (EBSD) technique. The results show that the surface of coatings prepared at current of 70~100 mA/cm2 is smooth and compact. Fracture mechanism of the Ni/W coatings is cleavage fracture. Thickness of the coatings increases with the increasing current density. Grain size and ratio of low angle grain boundaries of the coatings decrease with the increasing current density, and this is beneficial to obtaining the high performance of the coatings. © 2016, Editorial Office of Transactions of Materials and Heat Treatment. All right reserved.
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