Synthesis and crystal structure of 7-acetamido-5-chloro-8-(p- methyloxybenzenesulfonyloxy)-2-styrylquinoline - 文章详情页

作者：

Li, X.-M. (Li, X.-M..) | Zeng, C.-C. (Zeng, C.-C..) (学者：曾程初) | Jiao, Z.-G. (Jiao, Z.-G..) | Yan, H. (Yan, H..) (学者：严辉) | Zhong, R.-G. (Zhong, R.-G..) (学者：钟儒刚)

收录：

Scopus PKU CSCD

摘要：

The　title　compound　7-acetamido-5-chloro-8-(p-methyloxybenzenesulfonyloxy)-　2-styrylquinoline　4　(C26H21ClN2O5S,　Mr　=　508.96)　has　been　synthesized　and　characterized　by　H-NMR,　IR,　ESI-MS　and　single-crystal　X-ray　diffraction　techniques.　The　crystal　belongs　to　orthorhombic,　space　group　Pca21　with　a　=　7.920(3),　b　=　10.672(5),　c　=　28.008(12)　Å,　V　=　2367.3(17)　Å3,　Z=　4,　Dc=　1.415　g/cm3,　μ=　0.290　mm　1,　F(000)　=　1056,　R　=　0.0323　and　wR　=　0.0692　for　3895　unique　reflections　with　3127　observed　ones　(I　>　2σ(I)).　X-ray　analysis　reveals　that　the　styrylquinoline　subunit　adopts　a　coplanar　conformation,　where　the　benzene　ring　and　quinoline　are　in　trans　configuration.

关键词：

Crystal structure; Styrylquinoline derivatives; Synthesis

作者机构：

[ 1 ] [Li, X.-M.]College of Life Science and Bioengineering, Beijing University of Technology, Beijing 100022, China
[ 2 ] [Zeng, C.-C.]College of Life Science and Bioengineering, Beijing University of Technology, Beijing 100022, China
[ 3 ] [Jiao, Z.-G.]College of Life Science and Bioengineering, Beijing University of Technology, Beijing 100022, China
[ 4 ] [Yan, H.]College of Life Science and Bioengineering, Beijing University of Technology, Beijing 100022, China
[ 5 ] [Zhong, R.-G.]College of Life Science and Bioengineering, Beijing University of Technology, Beijing 100022, China

通讯作者信息：

曾程初
[Zeng, C.-C.]Majoring in Organic Synthesis and Organic Electrochemistry

电子邮件地址：

zengcc@bjut.edu.cn

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