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作者:

Ma, Shiyu (Ma, Shiyu.) | Zhang, Jianxin (Zhang, Jianxin.) | Li, Xueqiao (Li, Xueqiao.) | Mao, Shengcheng (Mao, Shengcheng.) (学者:毛圣成)

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EI Scopus SCIE

摘要:

High-resolution transmission electron microscopy was used to study interfacial characteristics between the plate-shaped sigma phase and the gamma phase in a Ni-based single crystal superalloy. The atomic structure of the sigma/gamma interface constituted by steps was presented. However, the HRTEM micrograph of sigma phase is not almost identical with the veritable atomic arrangement of sigma phase on the same zone axis. The image formation of HRTEM relies on phase contrast, instead of the amplification of the atomic arrangement. From the simulated HRTEM images, the approximate defocus and thickness of the sample can be got as - 3 nm and 6 nm sigma phase has the following crystallographic orientations relations with. matrix: [0 0 1]gamma//[1 1 2] sigma, (1 1 0)gamma//(1 -1 0) sigma, (-1 1 0)gamma//(1 1 -1) sigma, which can be proved by the stereographic projection. The interfacial steps are made up by (1 1 0)gamma and (-1 1 0)gamma or (1 -1 0) sigma and (1 1 -1) sigma. In the interface steps, the length of (-1 1 0)gamma//(1 1 -1) sigma is longer than (1 1 0)gamma//(1 -1 0) sigma, which is caused by that distortion factor of (-1 1 0)gamma//(1 1 -1) sigma is much smaller than that of (1 1 0)gamma//(1 -1 0) sigma.

关键词:

crystallographic orientations relation high-resolution transmission electron microscopy interface structure Ni-based single crystal superalloy sigma phase

作者机构:

  • [ 1 ] [Ma, Shiyu]Shandong Univ, Minist Educ, Key Lab Liquid Solid Struct Evolut & Proc Mat, Jinan 250061, Shandong, Peoples R China
  • [ 2 ] [Zhang, Jianxin]Shandong Univ, Minist Educ, Key Lab Liquid Solid Struct Evolut & Proc Mat, Jinan 250061, Shandong, Peoples R China
  • [ 3 ] [Li, Xueqiao]Beijing Univ Technol, Beijing Key Lab Microstruct & Property Adv Mat, Beijing 100024, Peoples R China
  • [ 4 ] [Mao, Shengcheng]Beijing Univ Technol, Beijing Key Lab Microstruct & Property Adv Mat, Beijing 100024, Peoples R China
  • [ 5 ] [Zhang, Jianxin]Shandong Univ, Sch Mat Sci & Engn, 17923 Jingshi Rd, Jinan 250061, Shandong, Peoples R China

通讯作者信息:

  • [Zhang, Jianxin]Shandong Univ, Minist Educ, Key Lab Liquid Solid Struct Evolut & Proc Mat, Jinan 250061, Shandong, Peoples R China;;[Zhang, Jianxin]Shandong Univ, Sch Mat Sci & Engn, 17923 Jingshi Rd, Jinan 250061, Shandong, Peoples R China

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来源 :

MATERIALS RESEARCH EXPRESS

ISSN: 2053-1591

年份: 2017

期: 11

卷: 4

2 . 3 0 0

JCR@2022

中科院分区:4

被引次数:

WoS核心集被引频次: 4

SCOPUS被引频次: 5

ESI高被引论文在榜: 0 展开所有

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