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摘要:
High-resolution transmission electron microscopy was used to study interfacial characteristics between the plate-shaped sigma phase and the gamma phase in a Ni-based single crystal superalloy. The atomic structure of the sigma/gamma interface constituted by steps was presented. However, the HRTEM micrograph of sigma phase is not almost identical with the veritable atomic arrangement of sigma phase on the same zone axis. The image formation of HRTEM relies on phase contrast, instead of the amplification of the atomic arrangement. From the simulated HRTEM images, the approximate defocus and thickness of the sample can be got as - 3 nm and 6 nm sigma phase has the following crystallographic orientations relations with. matrix: [0 0 1]gamma//[1 1 2] sigma, (1 1 0)gamma//(1 -1 0) sigma, (-1 1 0)gamma//(1 1 -1) sigma, which can be proved by the stereographic projection. The interfacial steps are made up by (1 1 0)gamma and (-1 1 0)gamma or (1 -1 0) sigma and (1 1 -1) sigma. In the interface steps, the length of (-1 1 0)gamma//(1 1 -1) sigma is longer than (1 1 0)gamma//(1 -1 0) sigma, which is caused by that distortion factor of (-1 1 0)gamma//(1 1 -1) sigma is much smaller than that of (1 1 0)gamma//(1 -1 0) sigma.
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来源 :
MATERIALS RESEARCH EXPRESS
ISSN: 2053-1591
年份: 2017
期: 11
卷: 4
2 . 3 0 0
JCR@2022
中科院分区:4