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Author:

Jing, G.-L. (Jing, G.-L..) | Tang, S. (Tang, S..) | Cli, X.-X. (Cli, X.-X..) | Wang, H.-Y. (Wang, H.-Y..)

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Abstract:

The silicon molybdbenum yellow method for spectrophotometry determination was applied to quantitative analyze silicon ion in ASP-flooding produced water. The effects of NaOH, polymer (HPAM) and sodium dodecylbenzene sulfonate (LAS) on quantitative analysis of silicon ions were discussed. The results showed that NaOH (0-7200 mg/L) and LAS (0-2400 mg/L) had almost no effect on the absorbance. Hydrochloric acid could be used to eliminate the influence of NaOH with high concentration (> 7200 mg/L). When the pH value was 1.2 and the dosage of HPAM (M=35 million) was between 0 and 80 mg/L, solution absorbance increased with increasing concentration of HPAM. The interference of polymer on the measuring of silicon ion could not be eliminated by adding 1 mL acetone, but it could be eliminated by diluting with distilled water. The interference of polymer with low molecular weight (M=3 million) and low concentration (0-40 mg/L) was weak. The method suggested was simple, rapid and of satisfactory precision and accuracy. The standard curve of linear regression equation was: A=0.0145c, and the correlation coefficient R2 was 0.9996. The linearity of absorbance concentration relationship maintained in the range of silicon ion concentration 0-20 mg/L. The accuracy of the method was less than 2%. The measured value of the relative standard deviation was only 1.39%, which indicated the repeatability of this method was good.

Keyword:

ASP-flooding; Oilfield produced water; Silicon ion; Silicon molybdbenum yellow method; Spectrophotometry

Author Community:

  • [ 1 ] [Jing, G.-L.]College of Environment and Energy Engineering, Beijing University of Technology, Beijing 100022, China
  • [ 2 ] [Jing, G.-L.]College of Chemistry and Chemical Engineering, Northeast Petroleum University, Daqing, Heilongjiang 163318, China
  • [ 3 ] [Tang, S.]College of Chemistry and Chemical Engineering, Northeast Petroleum University, Daqing, Heilongjiang 163318, China
  • [ 4 ] [Cli, X.-X.]College of Chemistry and Chemical Engineering, Northeast Petroleum University, Daqing, Heilongjiang 163318, China
  • [ 5 ] [Wang, H.-Y.]College of Chemistry and Chemical Engineering, Northeast Petroleum University, Daqing, Heilongjiang 163318, China

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Source :

Oilfield Chemistry

ISSN: 1000-4092

Year: 2013

Issue: 3

Volume: 30

Page: 457-459

Cited Count:

WoS CC Cited Count: 0

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 1

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