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摘要 ：
制备了金纳米粒子-氧化石墨烯(AuNPs-GO)复合物,采用透射电镜(TEM)和紫外-可见吸收光谱(UV-Vis)对其进行了表征。将此复合物修饰到玻碳电极(GCE)表面,再通过Au—S键将巯基修饰的富含鸟嘌呤的DNA链(T30695)自组装到电极表面的金纳米粒子上。T30695可与Pb~(2+)结合形成稳定的平行G-四链体,此G-四链体再与氯化血红素(Hemin)结合形成具有过氧化物酶活性的DNA酶(DNAzyme),基于此制得Pb~(2+)敏感的DNA酶电化学传感器。形成的DNA酶可催化H_2O_2氧化对苯二酚(HQ),实现电化学信号的放大和Pb~(2+)的高灵敏检测。在优化的实验条件下,在...
关键词 ：
DNA酶 DNA酶 方波伏安法 方波伏安法 铅离子(Ⅱ) 铅离子(Ⅱ) 传感器 传感器
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| GB/T 7714 | 杨瑞 , 康天放 , 鲁理平 et al. 基于DNA酶/AuNPs-GO传感器方波伏安法高灵敏检测Pb~(2+) [J]. | 分析化学 , 2021 , 49 (02) : 309-317 . |
| MLA | 杨瑞 et al. "基于DNA酶/AuNPs-GO传感器方波伏安法高灵敏检测Pb~(2+)" . | 分析化学 49 . 02 (2021) : 309-317 . |
| APA | 杨瑞 , 康天放 , 鲁理平 , 叶青 . 基于DNA酶/AuNPs-GO传感器方波伏安法高灵敏检测Pb~(2+) . | 分析化学 , 2021 , 49 (02) , 309-317 . |
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摘要 ：
The poisoning effects of alkali metals (K and Na) and alkaline earth metals (Ca and Mg) on catalytic performance of the 2Nb4Ce/Zr-PILC catalyst for the selective catalytic reduction of NOx with NH3 (NH3-SCR) were investigated, and physicochemical properties of the catalysts were characterized by means of the X-ray diffraction XRD (XRD), Brunner-Emmet-Teller (BET), hydrogen temperature-programmed reduction (H-2-TPR), X-ray Photoelectron Spectroscopy (XPS), ammonia temperature-programmed desorption (NH3-TPD), and in situ diffuse reflectance infrared Fourier transform spectroscopy (in situ DRIFTS) techniques. Doping of M (M = K, Na, Ca, and Mg) deactivated the 2Nb4Ce/Zr-PILC catalyst according to the sequence of 0.8 K > 0.8 Na > 0.8 Ca > 0.8 Mg (M/Ce molar ratio = 0.8). The characterization results showed that the decreases in redox ability, NH3 adsorption, Ce3+/Ce4+ atomic ratio, and amount of the chemisorbed oxygen (O-beta) were the important factors influencing catalytic activities of the alkali metal-and alkaline earth metal-doped samples. Consequently, compared with the Mg- and Ca-doped samples, doping of K caused the 2Nb4Ce/Zr-PILC sample to possess the lowest redox ability, NH3 adsorption, and amount of the O-beta species, which resulted in an obvious deactivation effect.
关键词 ：
alkali metal alkali metal alkaline earth metal alkaline earth metal NH3-SCR NH3-SCR poisoning poisoning selective catalytic reduction selective catalytic reduction surface acidity surface acidity
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| GB/T 7714 | Li, Chenxi , Cheng, Jin , Ye, Qing et al. Poisoning Effects of Alkali and Alkaline Earth Metal Doping on Selective Catalytic Reduction of NO with NH3 over the Nb-Ce/Zr-PILC Catalysts [J]. | CATALYSTS , 2021 , 11 (3) . |
| MLA | Li, Chenxi et al. "Poisoning Effects of Alkali and Alkaline Earth Metal Doping on Selective Catalytic Reduction of NO with NH3 over the Nb-Ce/Zr-PILC Catalysts" . | CATALYSTS 11 . 3 (2021) . |
| APA | Li, Chenxi , Cheng, Jin , Ye, Qing , Meng, Fanwei , Wang, Xinpeng , Dai, Hongxing . Poisoning Effects of Alkali and Alkaline Earth Metal Doping on Selective Catalytic Reduction of NO with NH3 over the Nb-Ce/Zr-PILC Catalysts . | CATALYSTS , 2021 , 11 (3) . |
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摘要 ：
To improve the removal capacity of (NO + O-2) effectively, the K-CMK-3(x) (KNO3: CMK-3 mass ratio (x) = 10-20 wt%, in which CMK-3 is an abbreviation of the ordered mesoporous carbon) samples were prepared, and their physical properties and (NO + O-2) adsorption performance were determined by means of analytical techniques, such as XRD, TEM, BET, TG, TPD, and DRIFTS. The ordered mesostructures were retained and specific surface areas and pore volumes of the K-CMK-3(x) samples increased after doping of K. Moreover, the doped K species were uniformly distributed on the surface of CMK-3, and K doping increased the amount of the basic sites in the sample. The structure and amount of the basic sites were the main factors influencing the (NO + O-2) adsorption on the sample. The sequence in (NO + O-2) adsorption performance was as follows: K-CMK-3(15) (143.8 mg/g) > K-CMK-3(20) (127.6 mg/g) > K-CMK-3(10) (103.6 mg/g) > CMK-3 (88.8 mg/g), with the K-CMK-3(15) sample possessing the best adsorption performance. There were two main adsorption pathways during the process of (NO + O-2) adsorption: one pathway was the conversion of NO and O-2 to a large number of NO2, in which part of NO2 was weakly adsorbed on the surface hydroxyl groups, and the other part of NO2 was disproportionated to NO, NO2-, and NO3-; and the other pathway was first the direct oxidization of NO to NO2- by the oxygen functional groups in carbon and then some of the formed NO2- species were converted to NO3-.
关键词 ：
Adsorption mechanism Adsorption mechanism CMK-3 CMK-3 (NO + O-2) adsorption (NO + O-2) adsorption Ordered mesoporous carbon Ordered mesoporous carbon Potassium doping Potassium doping
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| GB/T 7714 | Wu, Runping , Ye, Qing , Wu, Kai et al. Potassium-modified ordered mesoporous carbon materials (K-CMK-3): Highly efficient adsorbents for NO adsorption at low temperatures [J]. | JOURNAL OF SOLID STATE CHEMISTRY , 2021 , 294 . |
| MLA | Wu, Runping et al. "Potassium-modified ordered mesoporous carbon materials (K-CMK-3): Highly efficient adsorbents for NO adsorption at low temperatures" . | JOURNAL OF SOLID STATE CHEMISTRY 294 (2021) . |
| APA | Wu, Runping , Ye, Qing , Wu, Kai , Dai, Hongxing . Potassium-modified ordered mesoporous carbon materials (K-CMK-3): Highly efficient adsorbents for NO adsorption at low temperatures . | JOURNAL OF SOLID STATE CHEMISTRY , 2021 , 294 . |
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摘要 ：
As a heavy metal, Pb is one component in coal-fired flue gas and is widely considered to have a strong negative effect on catalyst activity in the selective catalytic reduction of NOx by NH3 (NH3-SCR). In this paper, we investigated the deactivation mechanism of the Mo-Ce/Zr-PILC catalyst induced by Pb in detail. We found that NO conversion over the 3Mo4Ce/Zr-PILC catalyst decreased greatly after the addition of Pb. The more severe deactivation induced by Pb was attributed to low surface area, lower amounts of chemisorbed oxygen species and surface Ce3+, and lower redox ability and surface acidity (especially a low number of Bronsted acid sites). Furthermore, the addition of Pb inhibited the formation of highly active intermediate nitrate species generated on the surface of the catalyst, hence decreasing the NH3-SCR activity.
关键词 ：
Mo-Ce/Zr-PILC catalyst Mo-Ce/Zr-PILC catalyst NH3-SCR NH3-SCR Pb poisoning Pb poisoning surface acidity surface acidity
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| GB/T 7714 | Li, Chenxi , Cheng, Jin , Ye, Qing et al. The Deactivation Mechanism of the Mo-Ce/Zr-PILC Catalyst Induced by Pb for the Selective Catalytic Reduction of NO with NH3 [J]. | NANOMATERIALS , 2021 , 11 (10) . |
| MLA | Li, Chenxi et al. "The Deactivation Mechanism of the Mo-Ce/Zr-PILC Catalyst Induced by Pb for the Selective Catalytic Reduction of NO with NH3" . | NANOMATERIALS 11 . 10 (2021) . |
| APA | Li, Chenxi , Cheng, Jin , Ye, Qing , Meng, Fanwei , Wang, Xinpeng , Dai, Hongxing . The Deactivation Mechanism of the Mo-Ce/Zr-PILC Catalyst Induced by Pb for the Selective Catalytic Reduction of NO with NH3 . | NANOMATERIALS , 2021 , 11 (10) . |
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摘要 ：
To improve the removal capacity of NO + O2 effectively, the alkaline earth metal-doped order mesoporous carbon (A-C-FDU-15(0.001) (A = Mg, Ca, Sr and Ba)) and Mg-C-FDU-15(x) (x = 0.001−0.003) samples were prepared, and their physicochemical and NO + O2 adsorption properties were determined by means of various techniques. The results show that the sequence in (NO + O2) adsorption performance was as follows: Mg-C-FDU-15(0.001) (93.2 mg/g) > Ca-C-FDU-15(0.001) (82.2 mg/g) > Sr-C-FDU-15(0.001) (76.1 mg/g) > Ba-C-FDU-15(0.001) (72.9 mg/g) > C-FDU-15 (67.1 mg/g). Among all of the A-C-FDU-15(0.001) samples, Mg-C-FDU-15(0.001) possessed the highest (NO + O2) adsorption capacity (106.2 mg/g). The species of alkaline earth metals and basic sites were important factors determining the adsorption of NO + O2 on the A-C-FDU-15(x) samples, and (NO + O2) adsorption on the samples was mainly chemical adsorption. Combined with the results of (NO + O2)-temperature-programmed desorption ((NO + O2)-TPD) and in situ diffused reflectance infrared Fourier transform spectroscopy (DRIFTS) characterization, we deduced that there were two main pathways of (NO + O2) adsorption: one was first the conversion of NO and O2 to NO2 and then part of NO2 was converted to NO2− and NO3−; and the other was the direct oxidation of NO to NO2− and NO3−. © 2020
关键词 ：
Adsorption Adsorption Alkaline earth metals Alkaline earth metals Alkalinity Alkalinity Fourier transform infrared spectroscopy Fourier transform infrared spectroscopy Nitrogen oxides Nitrogen oxides Physicochemical properties Physicochemical properties Temperature Temperature Temperature programmed desorption Temperature programmed desorption
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| GB/T 7714 | Wu, Runping , Ye, Qing , Wu, Kai et al. Low-temperature (NO + O2) adsorption performance of alkaline earth metal-doped C-FDU-15 [J]. | Journal of Environmental Sciences (China) , 2021 , 103 : 172-184 . |
| MLA | Wu, Runping et al. "Low-temperature (NO + O2) adsorption performance of alkaline earth metal-doped C-FDU-15" . | Journal of Environmental Sciences (China) 103 (2021) : 172-184 . |
| APA | Wu, Runping , Ye, Qing , Wu, Kai , Dai, Hongxing . Low-temperature (NO + O2) adsorption performance of alkaline earth metal-doped C-FDU-15 . | Journal of Environmental Sciences (China) , 2021 , 103 , 172-184 . |
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摘要 ：
研究了不同水热老化温度对钾(K)中毒0.4K-Cu-SAPO-18样品的结构及其NH3-SCR(NH3作为还原剂的选择性还原技术)催化活性的影响.结果表明,K中毒对样品结构影响较小,但明显降低了其NH3-SCR性能,在350℃时,K中毒样品0.4K-Cu-SAPO-18的NO转化率为65.88％,明显低于未中毒Cu-SAPO-18样品的90.85％.水热老化温度明显影响催化剂的结构,减少了活性位点,降低了表面酸性.随着水热老化温度升高,催化剂的AEI结构被破坏,活性物种数量降低,催化活性明显下降.氢气程序升温还原(H2-TPR)结果表明,孤立的Cu2+和Cu+的总量分别从未中毒Cu-SAPO-18样品的66.61和1.32μmol/g变化到K中毒0.4K-Cu-SAPO-18样品的39.52和101.96μmol/g,表明K中毒样品中孤立Cu2+容易转化为Cu2O.K中毒后,样品的弱酸、中强酸、强酸性位点的数量降低,分别从未中毒Cu-SAPO-18样品的0.201,0.103和0.302 mmol/g降低到中毒0.4K-Cu-SAPO-18样品的0.102,0.086和0.071 mmol/g.氨气程序升温脱附(NH3-TPD)和原位红外结果表明,K竞争性地取代了催化剂中孤立的Cu2+和H+,使K中毒0.4K-Cu-SAPO-18样品的活性位和酸性位减少,导致催化活性下降.在低温NH3-SCR反应中,K中毒和未中毒样品均以Eley-Rideal(E-R)和Langmuir-Hinshelwood(L-H)机理进行,而L-H机理占主导地位,但K中毒样品的反应速率明显降低.
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| GB/T 7714 | 孟繁伟 , 高琦 , 叶青 et al. Cu-SAPO-18催化剂氨选择性催化还原NOx钾中毒机理的研究 [J]. | 高等学校化学学报 , 2021 , 42 (9) : 2832-2841 . |
| MLA | 孟繁伟 et al. "Cu-SAPO-18催化剂氨选择性催化还原NOx钾中毒机理的研究" . | 高等学校化学学报 42 . 9 (2021) : 2832-2841 . |
| APA | 孟繁伟 , 高琦 , 叶青 , 李晨曦 . Cu-SAPO-18催化剂氨选择性催化还原NOx钾中毒机理的研究 . | 高等学校化学学报 , 2021 , 42 (9) , 2832-2841 . |
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摘要 ：
The Ni-loaded cryptomelane-type manganese oxide octahedral molecular sieve (OMS-2) catalysts (xNi/OMS-2: x = 1, 3, 5, and 10 wt%) were prepared by a pre-incorporation method. Physicochemical properties of the as-synthesized materials were characterized by means of various techniques, and their catalytic activities for CO, ethyl acetate, and toluene oxidation were evaluated.The loading of Ni played an important role in improving physicochemical propertiesof OMS-2. Among all of the samples, 5Ni/OMS-2 exhibited the best catalytic activity, with the T-90 being 155 degrees C for CO oxidation at a space velocity (SV) of 60,000 mL/(g center dot h), 225 degrees C for ethyl acetate oxidation at an SV of 240,000 mL/(g center dot h), and 300 degrees C for toluene oxidation at an SV of 240,000 mL/(g center dot h), which was due to its high Mn3+ content and O-ads concentration, good low-temperature reducibility and lattice oxygen mobility, and strong interaction between the Ni species and the OMS-2 support. In addition, catalytic mechanisms of the oxidation of three pollutants over 5Ni/OMS-2 were also studied. The oxidation of CO, ethyl acetate, and toluene over the catalysts took place first via the activated adsorption, then intermediates formation, and finally complete conversion of the formed intermediates to CO2 and H2O.
关键词 ：
CO oxidation CO oxidation cryptomelane-typemanganese oxide octahedral molecular sieve cryptomelane-typemanganese oxide octahedral molecular sieve ethyl acetate oxidation ethyl acetate oxidation supported nickel catalyst supported nickel catalyst toluene oxidation toluene oxidation
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| GB/T 7714 | Dong, Ning , Chen, Mengyue , Ye, Qing et al. Catalytic Elimination of Carbon Monoxide, Ethyl Acetate, and Toluene over the Ni/OMS-2 Catalysts [J]. | CATALYSTS , 2021 , 11 (5) . |
| MLA | Dong, Ning et al. "Catalytic Elimination of Carbon Monoxide, Ethyl Acetate, and Toluene over the Ni/OMS-2 Catalysts" . | CATALYSTS 11 . 5 (2021) . |
| APA | Dong, Ning , Chen, Mengyue , Ye, Qing , Zhang, Dan , Dai, Hongxing . Catalytic Elimination of Carbon Monoxide, Ethyl Acetate, and Toluene over the Ni/OMS-2 Catalysts . | CATALYSTS , 2021 , 11 (5) . |
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摘要 ：
The composite of gold nanoparticles-graphene oxide (AuNPs-GO) was prepared and characterized by transmission electron microscope (TEM) and ultraviolet-visible(UV-vis) spectrophotometry, respectively. The composite was modified on the surface of a glassy carbon electrode (GCE). The mercapto-modified and guanine-rich DNA strand (T30695) was self-assembled on to gold nanoparticles on the surface of the electrode via Au-S bond. T30695 could combine with lead ions (Pb2+) to form a stable parallel G-quadruplex. The G-quadruplex further combined with hemin to form DNAzyme with peroxidase activity. On the basis of this, DNAzyme electrochemical sensor Pb2+ detection was prepared. The DNAzyme could catalyze the oxidation reaction of hydrogen peroxidetowardshydroquinone (HQ) to achieve the amplification of electrochemical signal and highly sensitive detection of Pb2+. Under the optimum conditions, the peak current of square-wave voltammetry (SWV) was linearly dependent on the logarithm of Pb2+ concentration ranging from 5. 0 x10(-9) mol/L to 1. 0 x10(-6) mol/L with a detection limit of 1. 0 x10(-9) mol/L (S/N = 3). The recovery of Pb2+ in real water sample was 96% -105%. The sensor possessed good reproducibility, stability and selectivity to Pb2+.
关键词 ：
DNAzyme DNAzyme Lead ion (II) Lead ion (II) Sensor Sensor Square-wave voltammetry Square-wave voltammetry
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| GB/T 7714 | Yang Rui , Fang Tian-Fang , Lu Li-Ping et al. Highly Sensitive Detection of Pb2+ Based on DNAzyme/AuNPs-GO Sensor by Square-Wave Voltammetry [J]. | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY , 2021 , 49 (2) : 309-317 . |
| MLA | Yang Rui et al. "Highly Sensitive Detection of Pb2+ Based on DNAzyme/AuNPs-GO Sensor by Square-Wave Voltammetry" . | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 49 . 2 (2021) : 309-317 . |
| APA | Yang Rui , Fang Tian-Fang , Lu Li-Ping , Ye Qing . Highly Sensitive Detection of Pb2+ Based on DNAzyme/AuNPs-GO Sensor by Square-Wave Voltammetry . | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY , 2021 , 49 (2) , 309-317 . |
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摘要 ：
The porous carbon (CKC-X-Y, CKC is the corn kernel-derived carbon; Xis the activation temperature; and Y is the KOH/CKC mass ratio (2, 3, 4, and 5)) adsorbents were prepared from corn kernels by the KOH activation method. Textural property and oxygen functional group amount of the CKC-X-Y sample were influenced by the activator amount and activation temperature. Among the CKC-X-Y samples, the CKC-900-3 sample displayed the highest surface area (1943 m(2)/g) and the largest pore volume (1.10 cm(3)/g), whereas the CKC-900-4 sample possessed the highest amount (45.5 %) of oxygen functional groups. The CKC-900-4 sample exhibited the largest CO2 adsorption capacity (3.63 mmol/g at 25 degrees C) among all of the CKC-X-Y samples. The results indicate that the activated corn-derived porous biochar with a high surface area and a high oxygen functional groups amount possessed a large CO2 uptake. In addition, the CKC-X-Y samples showed high CO2/N-2 selectivity, good recyclability, and easy regeneration behavior. The adsorption of CO2 was physically and chemically adsorbed on the surface of the CKC-X-Y samples, with the physical adsorption being dominant. In which CO2 was mainly chemically adsorbed on the samples with hydroxyl groups.
关键词 ：
Adsorption kinetics Adsorption kinetics Adsorption mechanism Adsorption mechanism Carbon dioixde uptake Carbon dioixde uptake Corn kernel-derived porous carbon Corn kernel-derived porous carbon Oxygen functional group Oxygen functional group
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| GB/T 7714 | Wu, Runping , Ye, Qing , Wu, Kai et al. Highly efficient CO2 adsorption of corn kernel-derived porous carbon with abundant oxygen functional groups [J]. | JOURNAL OF CO2 UTILIZATION , 2021 , 51 . |
| MLA | Wu, Runping et al. "Highly efficient CO2 adsorption of corn kernel-derived porous carbon with abundant oxygen functional groups" . | JOURNAL OF CO2 UTILIZATION 51 (2021) . |
| APA | Wu, Runping , Ye, Qing , Wu, Kai , Wang, Lanyang , Dai, Hongxing . Highly efficient CO2 adsorption of corn kernel-derived porous carbon with abundant oxygen functional groups . | JOURNAL OF CO2 UTILIZATION , 2021 , 51 . |
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摘要 ：
Different Cu contents (x wt%) were supported on the cryptomelane-type manganese oxide octahedral molecular sieve (OMS-2) (xCu/OMS-2; x = 1, 5, 15, and 20) via a pre-incorporation method. Physicochemical properties of the OMS-2 and xCu/OMS-2 samples were characterized by means of the XRD, FT-IR, SEM, TG/DTG, ICP-OES, XPS, O-2-TPD, H-2-TPR, and in situ DRIFTS techniques, and their catalytic activities were measured for the oxidation of CO, ethyl acetate, and toluene. The results show that the Cu species were homogeneously dispersed in the tunnel and framework structure of OMS-2. Among all of the samples, 15Cu/OMS-2 sample exhibited the best activities with the T-50% of 65, 165, and 240 degrees C as well as the T-90% of 85, 215, and 290 degrees C for CO, ethyl acetate and toluene oxidation, respectively, which was due to the existence of the Cu species and Mn3+/Mn4+ redox couples, rich oxygen vacancies, good oxygen mobility, low-temperature reducibility, and strong interaction between the Cu species and the OMS-2 support. The reaction mechanisms were also deduced by analyzing the in situ DRIFTS spectra of the 15Cu/OMS-2 sample. The excellent oxygen mobility associated with the electron transfer between Cu species and Mn3+/Mn4+ redox couples might be conducive to the continuous replenishment of active oxygen species and the constantly generated reactant intermediates, thereby increasing the reactant reaction rate.
关键词 ：
carbon monoxide oxidation carbon monoxide oxidation cryptomelane-type manganese oxide cryptomelane-type manganese oxide OMS-2 OMS-2 supported CuOx catalysts supported CuOx catalysts volatile organic compounds oxidation volatile organic compounds oxidation
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| GB/T 7714 | Fu, Zhidan , Chen, Mengyue , Ye, Qing et al. Enhanced Performance of the OMS-2-Supported CuOx Catalysts for Carbon Monoxide, Ethyl Acetate, and Toluene Oxidation [J]. | CATALYSTS , 2021 , 11 (6) . |
| MLA | Fu, Zhidan et al. "Enhanced Performance of the OMS-2-Supported CuOx Catalysts for Carbon Monoxide, Ethyl Acetate, and Toluene Oxidation" . | CATALYSTS 11 . 6 (2021) . |
| APA | Fu, Zhidan , Chen, Mengyue , Ye, Qing , Dong, Ning , Dai, Hongxing . Enhanced Performance of the OMS-2-Supported CuOx Catalysts for Carbon Monoxide, Ethyl Acetate, and Toluene Oxidation . | CATALYSTS , 2021 , 11 (6) . |
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