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学者姓名：韩晓东
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摘要 ：
纳米Ir薄膜中缺陷结构的原子尺度研究
关键词 ：
缺陷 缺陷 多重孪晶 多重孪晶 面心立方 面心立方 位错 位错 原子尺度 原子尺度 孪晶界 孪晶界
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| GB/T 7714 | 韦如建 , 贺昕 , 王兴权 et al. 纳米Ir薄膜中缺陷结构的原子尺度研究 [J]. | 韦如建 , 2021 , 40 (2) : 101-107 . |
| MLA | 韦如建 et al. "纳米Ir薄膜中缺陷结构的原子尺度研究" . | 韦如建 40 . 2 (2021) : 101-107 . |
| APA | 韦如建 , 贺昕 , 王兴权 , 熊晓东 , 罗俊锋 , 闻明 et al. 纳米Ir薄膜中缺陷结构的原子尺度研究 . | 韦如建 , 2021 , 40 (2) , 101-107 . |
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摘要 ：
金属铱(Ir)因具有高密度,高熔点,高硬度等特点而被广泛应用于航空航天、军工等高新科技领域.但Ir的塑性差,严重影响其进一步广泛应用.金属自身的结构及缺陷对其力学性能具有重要影响,研究Ir的原子尺度微观结构可为其力学性能优化提供重要参考.本文主要利用透射电子显微镜(TEM)对纳米Ir薄膜中的缺陷类型和缺陷密度进行了研究.发现薄膜中存在高密度的孪晶以及位错.其中,薄膜中的孪晶密度为1.6×103(1/μm2).此外,研究还发现薄膜中有两大类缺陷的相互作用:位错与孪晶相互作用以及孪晶与孪晶相互作用.前者包括层错与孪晶相互作用以及全位错对孪晶的钉扎作用;孪晶之间的相互作用形态包括头对头对接式,三重孪晶和五重孪晶等多种形态.
关键词 ：
位错 位错 多重孪晶 多重孪晶 原子尺度 原子尺度 面心立方 面心立方 孪晶界 孪晶界 缺陷 缺陷
引用：
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| GB/T 7714 | 韦如建 , 贺昕 , 王兴权 et al. 纳米Ir薄膜中缺陷结构的原子尺度研究 [J]. | 电子显微学报 , 2021 , 40 (2) : 101-107 . |
| MLA | 韦如建 et al. "纳米Ir薄膜中缺陷结构的原子尺度研究" . | 电子显微学报 40 . 2 (2021) : 101-107 . |
| APA | 韦如建 , 贺昕 , 王兴权 , 熊晓东 , 罗俊锋 , 闻明 et al. 纳米Ir薄膜中缺陷结构的原子尺度研究 . | 电子显微学报 , 2021 , 40 (2) , 101-107 . |
| 导入链接 | NoteExpress RIS BibTex |
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| GB/T 7714 | Wang, Li , Li, Jintao , Zhang, Na et al. Investigations of EGFR configurations on tumor cell surface by high-resolution electron microscopy (vol 532, pg 179, 2020) [J]. | BIOCHEMICAL AND BIOPHYSICAL RESEARCH COMMUNICATIONS , 2021 , 558 : 239-239 . |
| MLA | Wang, Li et al. "Investigations of EGFR configurations on tumor cell surface by high-resolution electron microscopy (vol 532, pg 179, 2020)" . | BIOCHEMICAL AND BIOPHYSICAL RESEARCH COMMUNICATIONS 558 (2021) : 239-239 . |
| APA | Wang, Li , Li, Jintao , Zhang, Na , Zhang, Xiaofei , Xia, Yang , Chai, Binbin et al. Investigations of EGFR configurations on tumor cell surface by high-resolution electron microscopy (vol 532, pg 179, 2020) . | BIOCHEMICAL AND BIOPHYSICAL RESEARCH COMMUNICATIONS , 2021 , 558 , 239-239 . |
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摘要 ：
本文利用原位实验技术,在透射电镜中对AuAg纳米晶薄膜裂纹扩展以及裂纹前端塑性机制进行了原位原子尺度观察。原位观察发现,在初期,裂纹在晶界处形核并沿着晶界扩展,在裂纹前端晶粒内部有形变孪晶的形核与长大。随着应变的增加,逐渐转为穿晶断裂,此时晶粒内的生长孪晶及变形孪晶均展现出良好的塑性变形能力。本实验对人们理解面心立方合金纳米晶材料的裂纹扩展机制具有一定借鉴意义。
关键词 ：
合金 合金 孪晶 孪晶 晶间裂纹 晶间裂纹 纳米晶薄膜 纳米晶薄膜 裂纹扩展 裂纹扩展 退孪晶 退孪晶
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| GB/T 7714 | 杨成鹏 , 符立波 , 郭谊忠 et al. AuAg纳米晶薄膜裂纹扩展的原位原子尺度观察 [J]. | 电子显微学报 , 2021 , 40 (05) : 489-495 . |
| MLA | 杨成鹏 et al. "AuAg纳米晶薄膜裂纹扩展的原位原子尺度观察" . | 电子显微学报 40 . 05 (2021) : 489-495 . |
| APA | 杨成鹏 , 符立波 , 郭谊忠 , 王立华 , 张泽 , 韩晓东 . AuAg纳米晶薄膜裂纹扩展的原位原子尺度观察 . | 电子显微学报 , 2021 , 40 (05) , 489-495 . |
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摘要 ：
Organic-inorganic halide perovskites (OIHPs) have the typical composition of APbX(3), in which A is a cation such as methlyamine (MA) and formamidine (FA) and X is a halide anion such as Cl, Br, or I. The mixture at the A or X site in OIHPs provides greatly improved versatility in their compositions and therefore allows the enhancement of their performance in LEDs and solar cells. In real application circumstances and deformable devices, the mechanical properties of OIHPs are of great importance. In this work, the mechanical properties of three series of mixed OIHP single crystals, MAPbI(x)Br(3-x), MAPbBr(x)Cl(3-x), and FA(y)MA(1-y)PbBr(3), are studied by nanoindentation. The results are summarized according to the composition of these mixtures. With the increase in the FA content at the A site, the average Young's modulus (E) of FA(y)MA(1-y)PbBr(3) decreases greatly from 19.2 GPa to 11.5 GPa, which indicates that the influence of organic cations on the mechanical properties of OIHPs is as important as that of Pb-X bonds. The mixture at the A or X site could also increase the hardness (H) and the wear resistance (H/E ratio). The average values of hardness and wear resistance of MAPbI(0.1)Br(2.9) are almost double (0.63 GPa, 0.033) the values for undoped MAPbBr(3) (0.32 GPa, 0.017). The dynamic mechanical responses of the OIHP single crystals show reduced creep stress exponents and thus increased strain rate sensitivities in the mixture at the X site, thereby improving the ductility. The nanoindentation sites are characterized using a scanning electron microscope and slip bands are observed, suggesting the plastic deformation mechanism governed by the activation of dislocations.
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| GB/T 7714 | Ma, Lin , Li, Wanpeng , Yang, Kaixiang et al. A- or X-site mixture on mechanical properties of APbX(3) perovskite single crystals [J]. | APL MATERIALS , 2021 , 9 (4) . |
| MLA | Ma, Lin et al. "A- or X-site mixture on mechanical properties of APbX(3) perovskite single crystals" . | APL MATERIALS 9 . 4 (2021) . |
| APA | Ma, Lin , Li, Wanpeng , Yang, Kaixiang , Bi, Jianjun , Feng, Jicun , Zhang, Jiabei et al. A- or X-site mixture on mechanical properties of APbX(3) perovskite single crystals . | APL MATERIALS , 2021 , 9 (4) . |
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摘要 ：
We report an Ag1 single-atom catalyst (Ag1 /MnO2 ), which was synthesized from thermal transformation of Ag nanoparticles (NPs) and surface reconstruction of MnO2 . The evolution process of Ag NPs to single atoms is firstly revealed by various techniques, including in situ ETEM, in situ XRD and DFT calculations. The temperature-induced surface reconstruction process from the MnO2 (211) to (310) lattice plane is critical to firmly confine the existing surface of Ag single atoms; that is, the thermal treatment and surface reconstruction of MnO2 is the driving force for the formation of single Ag atoms. The as-obtained Ag1 /MnO2 achieved 95.7 % Faradic efficiency at -0.85 V vs. RHE, and coupled with long-term stability for electrochemical CO2 reduction reaction (CO2 RR). DFT calculations indicated single Ag sites possessed high electronic density close to Fermi Level and could act exclusively as the active sites in the CO2 RR. As a result, the Ag1 /MnO2 catalyst demonstrated remarkable performance for the CO2 RR, far surpassing the conventional Ag nanosized catalyst (AgNP /MnO2 ) and other reported Ag-based catalysts.
关键词 ：
anti-Ostwald ripening anti-Ostwald ripening CO2 reduction reaction CO2 reduction reaction silver silver surface reconstruction surface reconstruction
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| GB/T 7714 | Zhang Ningqiang , Zhang Xinxin , Tao Lei et al. Silver Single-Atom Catalyst for Efficient Electrochemical CO2 Reduction Synthesized from Thermal Transformation and Surface Reconstruction. [J]. | Angewandte Chemie , 2021 , 60 (11) : 6170-6176 . |
| MLA | Zhang Ningqiang et al. "Silver Single-Atom Catalyst for Efficient Electrochemical CO2 Reduction Synthesized from Thermal Transformation and Surface Reconstruction." . | Angewandte Chemie 60 . 11 (2021) : 6170-6176 . |
| APA | Zhang Ningqiang , Zhang Xinxin , Tao Lei , Jiang Peng , Ye Chenliang , Lin Rui et al. Silver Single-Atom Catalyst for Efficient Electrochemical CO2 Reduction Synthesized from Thermal Transformation and Surface Reconstruction. . | Angewandte Chemie , 2021 , 60 (11) , 6170-6176 . |
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摘要 ：
Understanding the high-temperature initial oxidation mechanism and its dynamic processes is generally important because a small amount of initial oxidation can induce rapid corrosion and cause catastrophic failure. We reveal the mechanism of initial oxidation in a third-generation Ni-based superalloy by in situ visualizations and investigations of the nano- and atomic-scale dynamic processes from room temperature to 900 degrees C with a Cs-corrected environmental transmission electron microscope. The initial oxidation starts from the gamma/gamma' interface at low temperatures. The high-temperature oxidation process with deficient oxygen prefers oxidation sites at the cross-junctions of the gamma/gamma' interfaces. The growth rate of the oxide nanoparticles depends on the oxidation temperatures, with a low rate below 600 degrees C and a rapid-growth speed at temperatures higher than 700 degrees C. Mass transfer from the gamma' and gamma phases to the gamma/gamma' interface, particularly at the cross-junctions of these interfaces, is observed to cause oxide accumulation. This study provides a direct observation of the interphase, interface-junction-initiated outward oxidization including Al and Cr elements. These results shed light on the initial oxidation mechanisms of materials containing a second phase with interphase interfaces and the materials at deficient oxygen conditions as well as those with protection coating layers. (C) 2021 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
关键词 ：
Dynamic mechanism Dynamic mechanism Interface Interface Junction Junction Nickel-based superalloy Nickel-based superalloy Oxidation Oxidation
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| GB/T 7714 | Zhai, Yadi , Chen, Yanhui , Zhao, Yunsong et al. Initial oxidation of Ni-based superalloy and its dynamic microscopic mechanisms: The interface junction initiated outwards oxidation [J]. | ACTA MATERIALIA , 2021 , 215 . |
| MLA | Zhai, Yadi et al. "Initial oxidation of Ni-based superalloy and its dynamic microscopic mechanisms: The interface junction initiated outwards oxidation" . | ACTA MATERIALIA 215 (2021) . |
| APA | Zhai, Yadi , Chen, Yanhui , Zhao, Yunsong , Long, Haibo , Li, Xueqiao , Deng, Qingsong et al. Initial oxidation of Ni-based superalloy and its dynamic microscopic mechanisms: The interface junction initiated outwards oxidation . | ACTA MATERIALIA , 2021 , 215 . |
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摘要 ：
Revealing the atomistic mechanisms for the high-temperature mechanical behavior of materials is important for optimizing their properties for service at high-temperatures and their thermomechanical processing. However, due to materials microstructure's dynamic recovery and the absence of available in situ techniques, the high-temperature deformation behavior and atomistic mechanisms of materials are difficult to evaluate. Here, we report the development of a microelectromechanical systems-based thermomechanical testing apparatus that enables mechanical testing at temperatures reaching 1556 K inside a transmission electron microscope for in situ investigation with atomic-resolution. With this unique technique, we first uncovered that tungsten fractures at 973 K in a ductile manner via a strain-induced multi-step body-centered cubic (BCC)-to-face-centered cubic (FCC) transformation and dislocation activities within the strain-induced FCC phase. Both events reduce the stress concentration at the crack tip and retard crack propagation. Our research provides an approach for timely and atomic-resolved high-temperature mechanical investigation of materials at high-temperatures.
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| GB/T 7714 | Zhang Jianfei , Li Yurong , Li Xiaochen et al. Timely and atomic-resolved high-temperature mechanical investigation of ductile fracture and atomistic mechanisms of tungsten. [J]. | Nature communications , 2021 , 12 (1) : 2218 . |
| MLA | Zhang Jianfei et al. "Timely and atomic-resolved high-temperature mechanical investigation of ductile fracture and atomistic mechanisms of tungsten." . | Nature communications 12 . 1 (2021) : 2218 . |
| APA | Zhang Jianfei , Li Yurong , Li Xiaochen , Zhai Yadi , Zhang Qing , Ma Dongfeng et al. Timely and atomic-resolved high-temperature mechanical investigation of ductile fracture and atomistic mechanisms of tungsten. . | Nature communications , 2021 , 12 (1) , 2218 . |
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摘要 ：
Photoelectronic performance of organic-inorganic hybrid perovskites has been investigated extensively. Advancement in optoelectronic characterization and application of this group of materials in solar cells, light-emitting diodes, and lasers has been pushed forward rapidly. However, nonlinear optical properties for applications in optical logic devices have not been exploited. Moreover, long-lived excitons and charges limit the response speed of such materials and further construction of ultrafast devices. In this work, we make use of the high third-order optical nonlinearity of (CH3NH3)PbBr3 single crystals and develop a femtosecond optical switch (OS) based on strong two-photon processes through absorbing one pump and one probe photon. The fascinating band structure, with a steep edge at 2.22 eV between the transmission and strong absorption bands, endows single crystals of (CH3NH3)PbBr3 with perfect characteristics for two-photon optical switching in the near infrared. An on-off ratio of the probe pulses of about 90% and a speed faster than 400 fs have been achieved for this OS device. To the best of our knowledge, such high efficiency has not been realized for an ultrafast OS with any other materials and devices. Moreover, this is a first exploration, to our best knowledge, of the third-order optical nonlinearity of organic-inorganic hybrid halide perovskites for application in ultrafast optical logic devices with high reliability and low threshold in the near infrared. (C) 2021 Optical Society of America under the terms of the OSA Open Access Publishing Agreement
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| GB/T 7714 | Zhang, Xinping , Wang, Meng , Ma, Lin et al. Ultrafast two-photon optical switch using single crystal hybrid halide perovskites [J]. | OPTICA , 2021 , 8 (5) : 735-742 . |
| MLA | Zhang, Xinping et al. "Ultrafast two-photon optical switch using single crystal hybrid halide perovskites" . | OPTICA 8 . 5 (2021) : 735-742 . |
| APA | Zhang, Xinping , Wang, Meng , Ma, Lin , Fu, Yulan , Guo, Jinxin , Ma, He et al. Ultrafast two-photon optical switch using single crystal hybrid halide perovskites . | OPTICA , 2021 , 8 (5) , 735-742 . |
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摘要 ：
Progress towards high performance X-ray detection and dynamic imaging applications, including nondestructive inspection, homeland security, and medical diagnostics, requires scintillators with a high light yield, a reasonable decay time, low cost, and eco-friendliness. Recently, copper halide scintillators have drawn tremendous attention due to their outstanding radioluminescence performance. Here, we first employed beta-Cs3Cu2Cl5 as a high-performance scintillator, with a photoluminescence quantum yield (PLQY) of 94.6%, a radioluminescence light yield of 34 000 +/- 4000 photons per MeV, a low detection limit of 81.7 nGy(air) s(-1), and good operational stability under a total X-ray dose of 174.6 Gy(air) in air. In addition, this scintillator presents a high spatial resolution of 9.6 lp mm(-1) at the modulation transfer function of 0.2 and a superb performance at 60 frames per second in our X-ray imaging system. Overall, this highly efficient scintillator demonstrates outstanding comprehensive performance and shows great potential for broad applications in X-ray detection and dynamic imaging.
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| GB/T 7714 | Zhou, Quan , Ren, Jiwei , Xiao, Jiawen et al. Highly efficient copper halide scintillators for high-performance and dynamic X-ray imaging [J]. | NANOSCALE , 2021 . |
| MLA | Zhou, Quan et al. "Highly efficient copper halide scintillators for high-performance and dynamic X-ray imaging" . | NANOSCALE (2021) . |
| APA | Zhou, Quan , Ren, Jiwei , Xiao, Jiawen , Lei, Lin , Liao, Feiyi , Di, Haipeng et al. Highly efficient copper halide scintillators for high-performance and dynamic X-ray imaging . | NANOSCALE , 2021 . |
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